Dissertations, Theses, and Capstone Projects

Date of Degree

9-2024

Document Type

Dissertation

Degree Name

Ph.D.

Program

Chemistry

Advisor

David R. Mootoo

Committee Members

Lynn Francesconi

Qiao Sheng Hu

Sheng P Zheng

Subject Categories

Chemistry | Organic Chemistry

Keywords

C-glycoside, Crotylation, Carbohydrate synthesis

Abstract

The involvement of carbohydrates in a plethora of fundamental biological pathways, including disease related processes, has created a demand for molecular probes for elucidating these mechanisms. Accordingly, synthesis of tailored and diverse carbohydrate-like molecules, commonly referred to as glycomimetics, is a very active area of research. Among the more popular classes of glycomimetics are C-glycosides, analogues in which the anomeric carbon of a parent sugar is attached to a carbon substituent. C-glycosides have attracted attention in the medicinal chemistry community as there are several naturally occurring examples with interesting pharmacologically activity. C-glycosides are also of interest because in contrast to their O-variants, they are hydrolytically stable and have different conformational properties. In this context, beyond the specific activity of certain analogues, there is a wider interest in C-glycosides as biomechanistic probes, and as stable derivatives of therapeutically interesting O-glycosides. Against this backdrop, the synthesis of C-glycosides is a very active area of research. Herein is described a review of recent developments in C-glycoside synthesis and the contributions of this thesis research to this field.

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